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Microtrac, Inc. has been a pioneer in light scattering particle
size technology for 30 years, and introduced the Ultrafine Particle
Analyzer in 1990. The newly enhanced and designed Nanotrac, features
faster measurements (up to 20 times faster), smaller particle size
capability (to 0.8 nm), higher precision, higher accuracy and advanced
software capabilities all in one small, robust dynamic light scattering
instrument having no moving components.
Rapid analysis – as fast as 15-30 seconds in most cases
Design – No moving parts and simple design means that that there
are no parts to wear nor be replaced
Chemical compatibility — Compatible with all organic solvents
ISO 13321 — Complies with this ISO standard on particle size measurements
for Dynamic Light Scattering
Brownian motion analysis — Advanced power spectrum analysis of Doppler
shifts by the Controlled Reference Method, patented by Microtrac,
Inc.
Temperature control – Precise temperature monitoring and compensation
eliminates need for temperature control baths or devices
High concentrations — This capability can eliminate concern of dilution,
a cause of agglomeration or dissolution
Low concentrations – As low as 0.1 ppm @200nm polystyrene
Operation simplicity – No advance knowledge of particle distribution
required — just add sample and measure
Security — Software compatible with FDA 21 CFR Part 11 for computer
and software security
Colored materials — Avoids multiple wavelength absorption issues
Physical size — Smallest dynamic light scattering footprint available
in particle size industry. Also available in a remote probe model
for external (“Dip ‘N’ Run”) measurement or for in line measurement
Accuracy – Mie scattering calculations for spherical particles and
proprietary modified Mie calculations for nonspherical particles.
Only Microtrac offers this enhanced accuracy for non-spherical particles
— the majority of real world materials
Range – Measurement capability from 0.0008 to 6.5 microns satisfies
most nanotechnology applications
Calibration – First principle optical physics avoids the need for
calibration – verification test kits are available. Alignment is
never needed
FDA Validation – Full documentation and personal customer support
Small sample size – Less than 3 ml per sample standard cell, or
as small as 0.1 ml with small cell option
Traceability — Particle size measurement traceable to NIST standards
Cost effective long term operation – The probe design avoids cost
of expendable cuvettes and pre-cleaning requirements; A background
measurement avoids need for ultra clean diluents
Applications — Organic polymers (latex polymers and others), nanometals
and other nanoinorganics, proteins, lipoproteins, DNA, and RNA
Data presentation — Accurately report narrow, monomodal, multimodal,
and broad range distributions in a variety of statistical formats
without the need to select special calculation algorithms
Resolution – Measures monomodal, multimodal, broad and narrow distributions
automatically without pre-selecting special programs
Consistency – Features afixed detector and laser design, which delivers
repeatability and linearity. High concentration capability avoids
agglomeration or dissolution of particles during dilution
Flexibility — The modular design allows selectable configurations
based on your application and can be expanded to meet future needs
at any time
Electronics — Advanced, high efficiency electronics for accurate
particle size measurements
Upgrades — Prior UPA models can be upgraded depending upon present
hardware and software
Power demand and safety — Low power laser provides electric and
laser irradiation safety
Versatility – Versions for the lab bench, on-line or even in-line
for process control applications
Reliability — Robust, rugged design assures reliable use for many
years into the future.
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Downloads
Nanotrac Literature
Microtrac
Flex Software Data Explanation Sheet
The Nanotrac® is currently available in two Models;
Both Nanotrac and Nanotrac Ultra are available in three configurations:
Internal cell, External Probe, or Versatile internal-external Combo
series.
State-of-the-art
technology:
The Nanotrac uses a newer, advanced power spectrum analysis
of Doppler shifts to produce a full volume distribution of particle
sizes. spectrum of particle sizes provided as a particle size distribution
of volume (mass) percent and intensity. While other systems measure
the light after it has passed through a sample, and at one or more
angles, Nanotrac uses a reference beam and backscatter optics to
insure minimum penetrate of light into the sample. Light undergoing
Frequency shifted scattered light collected at minimum sample penetration
avoids multiple scattering effects. Scattered light caused by interaction
with randomly moving particles is mixed with a portion of the original
laser after being reflected back into the probe at 180 degrees.
The combined light passes through a fiber-optic cable to a single
detector, and advanced electronics and software analyze the signals
to calculate the Doppler shifts corresponding to particle size.
Controlled Reference Method technology, in which mixing of the laser
and scattered light occur, provides high signals using low power.
Small size semiconductor lasers provide extremely long life and
safety. No moving parts and no maintenance assures that the Nanotrac
will reliably provide data for years without concern for repeat
service visits. Advanced calculations avoid the ambiguity of polydispersity
(PDI) index while providing measured distribution shape. Calculation
of the full particle size distribution avoids the ambiguity of distribution
approximation methods assuring you maximum size information about
your particle suspension.
Condensed Specifications:
Range and Spec
0.8 to 6500 nanometers (0.0008 to 6.5 microns)
Repeatability
1% for 100nm polystyrene
Optics/Alignment
Fixed laser and detector positions; 780 nm semiconductor laser directed
to sample through a fiber optic cable. Alignment of optics never
needed
Measurement Angle
180 Degrees
Complete System
Solid-state optical bench, Pentium IV computer, CRT or flat screen
monitor, complete data management software, printer options
Data Handling
Advanced Microtrac FLEX Software offers unparalleled capability
for graphics, data export/import, customized printed reports, and
all data handling demands including export to Adobe PDF, as well
as other export formats for sharing data over the internet. FLEX
software provides data storage in Microsoft Access® database
format utilizing OLE. Volume, number, area and intensity weighted
distributions as well as percentile and other summary data. Data
integrity is ensured using FDA 21CFR Part 11 compliant security
features.
Sample Handling
Powders, fluids and all particles suspended or suspendable in fluid.
Manual transfer and rinsing of sample for Nanotrac 150.
Sample size – Less than 3 ml or as low as 0.1ml with small cell
option. Samples may be measured by dipping probe directly into sample
using Nanotrac 250.
Suspending Medium
Compatible with any organic solvent and most acids and bases generally
used to deliver particulate samples
Power Requirements
90 to 240 VAC, 5 amps, 47/63 Hz, single phase
Dimensions
Height: 13 in. (33.0 cm); Width: 22 in. (55.9 cm); Depth: 12 in.
(30.5 cm) not including computer or UAC 112
Typical Analysis Time
30 to 120 seconds
Delivery System
None required
Mode of Operation
Independent, manual operation or fully automatic control using the
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